Аннотация:The analysis of the kinetics of stepwise bulk crystallization of AsSe1.5In0.01 glasses at temperatures of 200, 220, 240, and 260°C and AsSe1.5In0.025 at 240°C has been carried out using the data of density measurements of quenched materials with the use of the generalized Kolmogorov-Avrami equation, the results of differential thermal and quantitative X-ray phase analysis, and microscopic observations. A significant acceleration of volumetric heterogeneous nucleation of plate-like crystals of the main phase As2Se3 by the primary microphase In2Se3, isolated uniformly throughout the volume of monolithic glass at isothermal crystallization in the range of 200-260°C, has been established. The parameters of specific electrical conductivity and microhardness of quenched semiconductor silals at different stages of heat treatment have been investigated