Properties of a granulated nitrogen-doped graphene oxide aerogelстатья
Статья опубликована в высокорейтинговом журнале
Информация о цитировании статьи получена из
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Scopus
Статья опубликована в журнале из списка Web of Science и/или Scopus
Дата последнего поиска статьи во внешних источниках: 26 декабря 2018 г.
Аннотация:At first, a granulated aerogel of graphene oxide was obtained, which was later reduced by hydrazine vapour. The
reduced aerogel was characterized through elemental analysis, infrared (IR) and Raman spectroscopy, electron
paramagnetic resonance (EPR), thermogravimetric analyses (TGA), voltammetry, and X-ray photoelectron
spectroscopy (XPS). Furthermore, the reduced sample was found to contain approximately 3 wt.% of nitrogen,
which was present in the aerogel in three states corresponding to the photoelectron peaks N1s with binding
energies of 399.5, 401.3, and 403.6 eV. In the electroreduction of oxygen, an appreciable catalytic effect was
observed for the sample under study, which resulted from reducing the overvoltage of the reaction by ~90 mV
and changing the mechanism of reduction.